Efficient Synthesis of Azo Dye Labeled Terpenes, Sugars, and Steroids Using N-(4-Arylazobenzoyl)-1H-benzotriazoles

被引：8

作者：

Katritzky, Alan R. ^{[1
]}

Tala, Srinivasa R. ^{[1
]}

Abo-Dya, Nader E. ^{[1
,2
]}

Abdel-Samii, Zakaria K. ^{[2
]}

机构：

[1] Univ Florida, Dept Chem, Ctr Heterocycl Cpds, Gainesville, FL 32611 USA

[2] Zagazig Univ, Fac Pharm, Dept Organ Pharmaceut Chem, Zagazig 44519, Egypt

来源：

SYNTHESIS-STUTTGART | 2009年 / 10期

关键词：

azo dyes; acylations; steroids; sugars; terpenes; AMINO-ACIDS; DERIVATIVES; FMOC-ALPHA-AMINOACYL)BENZOTRIAZOLES; ACYLBENZOTRIAZOLES; CHOLESTEROL; REAGENTS; BEHAVIOR; BINDING;

D O I：

10.1055/s-0029-1216786

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

N-(4-Arylazobenzoyl)-1H-benzotriazoles react with hydroxyterpenes, sugars, and steroids in the presence of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) at room temperature in tetrahydrofuran to afford azo dye labeled terpenes, sugars, and steroids (45-82% yield).

引用

页码：1708 / 1714

页数：7

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