The crystal structure of 2-benzoylpyridine N4-methyl-N4-phenylthiosemicarbazone

被引：8

作者：

ValdesMartinez, J ^{[1
]}

HernandezOrtega, S ^{[1
]}

West, DX ^{[1
]}

Stark, AM ^{[1
]}

Bain, GA ^{[1
]}

机构：

[1] ILLINOIS STATE UNIV, DEPT CHEM, NORMAL, IL 61790 USA

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 1996年 / 26卷 / 12期

关键词：

thiosemicarbazone; 2-benzoylpyridine; N4-substituted; hydrogen bonding;

D O I：

10.1007/BF01670320

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

2-Benzoylpyridine N4-methyl-N4-phenylthiosemicarbazone, HBz4MePh, monoclinic, P2(1)/n, a = 9.141(2), b = 18.507(4), c = 11.401(2) Angstrom, beta = 110.58(3)degrees, V = 1805.6(9) Angstrom(3), Z = 4, mu = 1.655 mm(-1). HBz4MePh crystallizes in a hydrogen bonded Z isomeric conformation with respect to the C7-N2 bond. The intramolecular hydrogen bond is between N3-H ... N1, and the S atom is Z to the azomethine nitrogen, N2.

引用

页码：861 / 864

页数：4

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