Separation, identification and determination of sanguinarine in argemone and other adulterated edible oils by reversed-phase high-performance liquid chromatography

被引:23
作者
Husain, S [1 ]
Narsimha, R [1 ]
Rao, RN [1 ]
机构
[1] Indian Inst Chem Technol, Analyt Chem & Environm Sci Div, Hyderabad 500007, Andhra Pradesh, India
关键词
oils; argemone oil; sanguinarine; alkaloids; benzophenanthridine;
D O I
10.1016/S0021-9673(99)00964-4
中图分类号
Q5 [生物化学];
学科分类号
071010 [生物化学与分子生物学]; 081704 [应用化学];
摘要
A simple, rapid and reliable reversed-phase high-performance liquid chromatographic method for the separation and determination of sanguinarine in argemone and other edible oils has been developed. The separation has been achieved on a C-18 column with CH3OH-CH3CN-tetrahydrofuran-water as mobile phase using diode array detection at 280 nm. The minimum detection limit of sanguinarine in the adulterated edible oils is 5 mu g/g. (C) 1999 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:123 / 126
页数:4
相关论文
共 11 条
[1]
EHMEKE HU, 1979, FRESEN Z ANAL CHEM, V294, P251
[2]
GOVE PB, 1961, WEBSTERS 3 NEW INT D, P2011
[3]
DISTRIBUTION OF CERTAIN POPPY-FUMARIA ALKALOIDS AND A POSSIBLE LINK WITH INCIDENCE OF GLAUCOMA [J].
HAKIM, SA ;
MIJOVIC, V ;
WALKER, J .
NATURE, 1961, 189 (476) :198-&
[4]
REVERSED-PHASE LIQUID-CHROMATOGRAPHY OF AROMATIC SULFONIC-ACIDS AND OTHER STRONGLY POLAR COMPOUNDS WITHOUT ADDITION OF AN ION-PAIRING COUNTERION [J].
JANDERA, P ;
CHURACEK, J .
JOURNAL OF CHROMATOGRAPHY, 1980, 197 (02) :181-187
[5]
THE BENZOPHENANTHRIDINE ALKALOIDS [J].
KRANE, BD ;
FAGBULE, MO ;
SHAMMA, M ;
GOZLER, B .
JOURNAL OF NATURAL PRODUCTS, 1984, 47 (01) :1-43
[6]
ISOLATION, CHEMISTRY AND BIOLOGY OF ALKALOIDS FROM PLANTS OF THE PAPAVERACEAE .84. ANTI-INFLAMMATORY ACTIVITY OF QUATERNARY BENZOPHENANTHRIDINE ALKALOIDS FROM CHELIDONIUM-MAJUS [J].
LENFELD, J ;
KROUTIL, M ;
MARSALEK, E ;
SLAVIK, J ;
PREININGER, V ;
SIMANEK, V .
PLANTA MEDICA, 1981, 43 (02) :161-165
[7]
MADHAVAN A, 1998, J OIL TECH ASS IND, V30, P181
[8]
SANGUINARINE LEVELS IN BIOLOGICAL SAMPLES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].
REINHART, P ;
HARKRADER, R ;
WYLIE, R ;
YEWEY, G ;
VANHORNE, KC .
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1991, 570 (02) :425-434
[9]
SHENOLIKAR IS, 1981, INDIAN J MED RES, V73, P204
[10]
THORNE EM, 1986, J SOC COSMET CHEM, V37, P279