Versatile, low-volume, thin-layer cell for in situ spectroelectrochemistry

被引：26

作者：

MosierBoss, PA ^{[1
]}

Newbery, R ^{[1
]}

Szpak, S ^{[1
]}

Lieberman, SH ^{[1
]}

Rovang, JW ^{[1
]}

机构：

[1] 3M COLUMBIA,COLUMBIA,MO 65202

来源：

ANALYTICAL CHEMISTRY | 1996年 / 68卷 / 18期

关键词：

D O I：

10.1021/ac960084n

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The design of a versatile, thin-layer cell to perform in situ spectroelectrochemistry is discussed, The cell is low-volume, leak-tight, and easily disassembled. It is constructed of chemically resistant materials and can be used to probe the electrochemical reactions of corrosives as well as moisture- and air-sensitive materials. The use of this cell to monitor the electrochemical reactions of oxyhalide electrolytes by in situ infrared spectroelectrochemistry and pyridine by surface-enhanced Raman scattering spectroscopy is demonstrated.

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收藏

页码：3277 / 3282

页数：6

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