Atomic resolution on small three-dimensional metal clusters by STM

被引:64
作者
Piednoir, A [1 ]
Perrot, E [1 ]
Granjeaud, S [1 ]
Humbert, A [1 ]
Chapon, C [1 ]
Henry, CR [1 ]
机构
[1] FAC SCI LUMINY,GPEC,F-13288 MARSEILLE,FRANCE
关键词
clusters; palladium; scanning tunneling microscopy;
D O I
10.1016/S0039-6028(97)00419-6
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Small, three-dimensional Pd clusters (d < 5 nm) deposited under UHV on two different single crystal surfaces (graphite and MoS2) are imaged with atomic resolution, both in air and in UHV, using scanning tunneling microscopy (STM). We show that a complete characterization of the morphology of the cluster can be achieved: three-dimensional shape; azimuthal orientation on the substrate; and arrangement of atoms on lateral facets. These results are in good agreement with those obtained from TEM observations on large particles (d > 10 nm). Some limitations of STM for such studies are discussed. (C) 1997 Elsevier Science B.V.
引用
收藏
页码:19 / 26
页数:8
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