Preparation of BaTiO3 nanoparticles by combustion spray pyrolysis

被引:29
作者
Lee, S
Son, T
Yun, JD
Kwon, H
Messing, GL
Jun, B
机构
[1] Kyungnam Univ, Div Adv Mat Engn, Masan 631701, South Korea
[2] Penn State Univ, Dept Mat Sci & Engn, University Pk, PA 16802 USA
关键词
BaTiO3; nanomaterials; spray pyrolysis; combustion; powder technology;
D O I
10.1016/j.matlet.2004.05.022
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
BaTiO3 nanoparticles were synthesized by combustion spray pyrolysis using a 1:1 molar ratio of oxidizer and fuel. To prepare solution precursor, Ba(NO3)(2), TiO(NO3)(2), CH6N4O, and NH4NO3 with the molar ratio of 1:1:4:2.75 were mixed in distilled water with 10% ethyl alcohol. A 0.01 M solution was ultrasonically sprayed into a quartz tube heated at 800 degreesC. The number concentration of droplets was decreased and large particles were removed by passing the droplets through a metal screen filter. The synthesized particles were well crystallized tetragonal BaTiO3. The median diameter of BaTiO3 was 60 nm. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:2932 / 2936
页数:5
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