In situ studies of the sol-gel synthesis of materials

被引:127
作者
Cheetham, AK
Mellot, CF
机构
[1] Materials Research Laboratory, University of California, Santa Barbara
关键词
D O I
10.1021/cm970497k
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The use of in situ methods to study the synthesis of materials from sol-gel precursors is reviewed, with particular emphasis on the formation of crystalline phases from solid gel precursors and the crystallization of zeolitic materials from solution under hydrothermal conditions. A wide range of studies that have been performed under nonambient conditions are discussed under the following headings: X-ray and neutron methods, spectroscopic and resonance methods, and imaging methods. Some current trends and future developments are assessed.
引用
收藏
页码:2269 / 2279
页数:11
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