A room-temperature synthesis of titanium nitride hollow spheres

被引：17

作者：

Chen, LY

Gu, YL

Shi, L

Ma, JH

Yang, Z

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem, Anhua 230026, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Anhua 230026, Peoples R China

来源：

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY | 2004年 / 4卷 / 07期

关键词：

titanium nitride; hollow spheres; chemical synthesis; X-ray diffraction; transmission electron microscopy;

D O I：

10.1166/jnn.2004.115

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Titanium nitride hollow spheres were synthesized by the reaction of TiCl4 and NaNH2 at room temperature. X-ray powder diffraction (XRD) pattern could be indexed as cubic TiN with the lattice constants of a = 4.236 Angstrom. Transmission electron microscopy (TEM) images showed hollow spheres with diameter about 200 nm. A possible formation mechanism of TiN hollow spheres was discussed.

引用

收藏

页码：896 / 898

页数：3

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