Development of a robust method for the quantitative determination of disaccharides in honey by gas chromatography

被引：32

作者：

de la Fuente, E. ^{[1
]}

Sanz, M. L. ^{[1
]}

Martinez-Castro, I. ^{[1
]}

Sanz, J. ^{[1
]}

机构：

[1] CSIC, Inst Quim Organ Gen, E-28006 Madrid, Spain

来源：

JOURNAL OF CHROMATOGRAPHY A | 2006年 / 1135卷 / 02期

关键词：

honey; disaccharides; gas chromatography; quantitative analysis;

D O I：

10.1016/j.chroma.2006.09.035

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

An iterative method for the GC quantitative determination of TMS-oxime disaccharides in honey has been developed. This approach takes into account possible positive systematic errors caused by unidentified compounds which overlap with the expected disaccharides. The results of its application to the determination of 15 disaccharides in simulated honey samples indicate that the iterative method is more robust that methods based on least-squares regression, improves the accuracy of the quantitative analysis and allows to detect the possible presence of disaccharides not identified. (c) 2006 Elsevier B.V. All rights reserved.

引用

页码：212 / 218

页数：7

共 21 条

[1] Optimization of the capillary gas chromatographic analysis of mono- and oligosaccharides in honeys [J].