Simultaneous soft X-ray transmission and emission microscopy

被引:90
作者
Gianoncelli, A. [1 ]
Kaulich, B. [1 ]
Alberti, R. [2 ,3 ]
Klatka, T. [2 ,3 ]
Longoni, A. [2 ,3 ]
de Marco, A. [4 ]
Marcello, A. [4 ]
Kiskinova, M. [1 ]
机构
[1] ELETTRA Sincrotrone Trieste, Xray Microscopy Sect, I-34012 Trieste, Italy
[2] Politecn Milan, Dipartimento Elettron & Informaz, I-23100 Milan, Italy
[3] Ist Nazl Fis Nucl, Sez Milano, I-20133 Milan, Italy
[4] ICGEB, Dept Mol Virol, I-34012 Padriciano, Italy
关键词
X-ray fluorescence; Soft X-ray microscopy; Carbon edge; SILICON DRIFT DETECTORS; RESOLUTION; SPECTROSCOPY; MICROPROBE; BEAMLINE; OPTICS; CELLS;
D O I
10.1016/j.nima.2009.06.035
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Novel low-energy X-ray fluorescence (LEXRF) system based on a multiple Si drift detector (SDD) configuration has been developed and implemented in the European TwinMic X-ray microspectroscopy station operating at the Italian synchrotron radiation facility ELETTRA. The setup, hosting up to eight large-area SDDs with specially adapted readout electronics, has demonstrated excellent performance for elemental analysis in the 280-2200eV photon energy range, which covers the K and L edges of light elements, starting from C. The great advantage is the simultaneous acquisition of LEXRF, absorption and phase contrast maps, providing complementary information on elemental composition and morphology of specimen at submicrometer length scales. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:195 / 198
页数:4
相关论文
共 21 条
[1]  
ANDRE CG, 1978, M CRIS VIEW LUN 24 H
[2]  
Bianco A., 2005, SPIE, V5918
[3]   Applications of synchrotron-based micro-imaging techniques to the chemical analysis of ancient paintings [J].
Cotte, Marine ;
Susini, Jean ;
Sole, V. Armando ;
Taniguchi, Yoko ;
Chillida, Javier ;
Checroun, Emilie ;
Walter, Philippe .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 2008, 23 (06) :820-828
[4]   Integrating Silicon detector with segmentation for scanning transmission X-ray microscopy [J].
Feser, Michael ;
Hornberger, Benjamin ;
Jacobsen, Chris ;
De Geronimo, Gianluigi ;
Rehak, Pavel ;
Holl, Peter ;
Strueder, Lothar .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2006, 565 (02) :841-854
[5]   LUCIA, a microfocus soft XAS beamline [J].
Flank, AM ;
Cauchon, G ;
Lagarde, P ;
Bac, S ;
Janousch, M ;
Wetter, R ;
Dubuisson, JM ;
Idir, M ;
Langlois, F ;
Moreno, T ;
Vantelon, D .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2006, 246 (01) :269-274
[6]   The quantum efficiency of pn-detectors from the near infrared to the soft X-ray region [J].
Hartmann, R ;
Stephan, KH ;
Strüder, L .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2000, 439 (2-3) :216-220
[7]  
Janssens K.H. A., 2000, MICROSCOPIC XRAY FLU
[8]   FIRST EXPERIMENTAL RESULTS FROM IBM/TENN/TULANE/LLNL/LBL UNDULATOR BEAMLINE AT THE ADVANCED LIGHT-SOURCE [J].
JIA, JJ ;
CALLCOTT, TA ;
YURKAS, J ;
ELLIS, AW ;
HIMPSEL, FJ ;
SAMANT, MG ;
STOHR, J ;
EDERER, DL ;
CARLISLE, JA ;
HUDSON, EA ;
TERMINELLO, LJ ;
SHUH, DK ;
PERERA, RCC .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1995, 66 (02) :1394-1397
[9]   MICRO-PIXE ANALYSIS OF MACRO ELEMENTS AND TRACE-ELEMENTS IN BLOOD-CELLS AND TUMORS OF PATIENTS WITH BREAST-CANCER [J].
JOHANSSON, E ;
LINDH, U ;
JOHANSSON, H ;
SUNDSTROM, C .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1987, 22 (1-3) :179-183
[10]   Differential interference contrast x-ray microscopy with twin zone plates [J].
Kaulich, B ;
Wilhein, T ;
Di Fabrizio, E ;
Romanato, F ;
Altissimo, M ;
Cabrini, S ;
Fayard, B ;
Susini, J .
JOURNAL OF THE OPTICAL SOCIETY OF AMERICA A-OPTICS IMAGE SCIENCE AND VISION, 2002, 19 (04) :797-806