The influence of a heat treatment on the microstructure and mechanical properties of sputtered coatings

被引:92
作者
Herr, W
Broszeit, E
机构
[1] Technician Sch Weilburg, Dept Mech, D-35781 Weilburg, Germany
[2] Tech Univ Darmstadt, Inst Mat Sci, D-64283 Darmstadt, Germany
关键词
heat treatment; sputtering; PVD; Auger electron spectroscopy; intrinsic stress; microhardness; adhesion; microstructure; nitrides; borides;
D O I
10.1016/S0257-8972(97)00196-5
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The aim of this paper was to examine correlations between deposition parameters and the coating properties of RF-sputtered films in deposition conditions and after heat treatment at temperatures up to 700 degrees C. The investigations deal with titanium-, chromium- and hafnium-based nitrides, borides and ternary alloys. Different materials such as SAE 52100 steel, ASP 23 highspeed steel and Ti6Al4V titanium alloy, which are commonly used in the aerospace industry, were coated to analyse the influence of the substrate material. The coatings were tested with respect to their phase composition, microstructure, residual stress, thickness, microhardness and adhesion. It is shown that the deposition parameters, as well as heat treatment at a temperature as low as 400 degrees C, can change considerably the coating properties. (C) 1997 Elsevier Science S.A.
引用
收藏
页码:335 / 340
页数:6
相关论文
共 7 条
  • [1] HALL EO, 1970, YIELD POINT PHENOMEN
  • [2] INFLUENCE OF SUBSTRATE MATERIAL AND DEPOSITION PARAMETERS ON THE STRUCTURE, RESIDUAL-STRESSES, HARDNESS AND ADHESION OF SPUTTERED CRXNY HARD COATINGS
    HERR, W
    MATTHES, B
    BROSZEIT, E
    MEYER, M
    SUCHENTRUNK, R
    [J]. SURFACE & COATINGS TECHNOLOGY, 1993, 60 (1-3) : 428 - 433
  • [3] HERR W, 1997, SURF COAT TECHNOL
  • [4] HERR W, 1996, THESIS TH DARMSTADT
  • [5] ANALYSIS OF RF-SPUTTERED TIB2 HARD COATINGS BY MEANS OF X-RAY-DIFFRACTOMETRY AND AUGER-ELECTRON SPECTROSCOPY
    LOHMANN, R
    OSTERSCHULZE, E
    THOMA, K
    GARTNER, H
    HERR, W
    MATTHES, B
    BROSZEIT, E
    KLOOS, KH
    [J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1991, 139 : 259 - 263
  • [6] HIGH-RESOLUTION AUGER-ELECTRON SPECTROSCOPY FOR CHARACTERIZATION OF SOLID COATINGS
    NOLD, E
    ADELHELM, C
    HOLLECK, H
    [J]. MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK, 1990, 21 (03) : 137 - 139
  • [7] POLLOCK HM, 1986, ASTM SPEC TECH PUB, V889, P47