Fluorination of 2-oxo-ethane derivatives with diethylaminosulfur trifluoride (DAST)

被引：23

作者：

Hagele, G

Haas, A

机构：

[1] Inst. of Inorg. Chem./Struct. Chem., Heinrich-Heine Univ. Dusseldorf, D-40225 Düsseldorf

来源：

JOURNAL OF FLUORINE CHEMISTRY | 1996年 / 76卷 / 01期

关键词：

diethylaminosulfur trifluoride; difluoromethylene compounds; ZnI2; catalyst; NMR spectroscopy; 2-Oxo-ethane derivatives;

D O I：

10.1016/0022-1139(95)03346-7

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The fluorination of 2-oxo-ethane derivatives with DAST is described. The use of ZnI2 as a catalyst improves the yield in the fluorination of 2-phenyl-2-oxo-acetonitrile with DAST.

引用

页码：15 / 19

页数：5

共 23 条

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