Isolation and characterization of limonoate and nomilinoate A-ring lactones

被引:27
作者
Zukas, AA [1 ]
Breksa, AP [1 ]
Manners, GD [1 ]
机构
[1] United States Dept Agr, Western Reg Res Ctr, Agr Res Serv, Albany, CA 94710 USA
关键词
Citrus glandis; Rutaccae; limonoids; limonoate A-ring lactone; nomilinoate A-ring lactone;
D O I
10.1016/j.phytochem.2004.08.016
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 [生物化学与分子生物学]; 081704 [应用化学];
摘要
A method combining solid-phase extraction and reversed-phase high-performance liquid chromatography is described for the isolation of two key metabolites in the limonoid biosynthetic pathway critical to citrus quality. Potassium salts of limonoate A-ring lactone and nomilinoate A-ring lactone were isolated from young Chandler pummelo seedlings and characterized on the basis of proton and carbon NMR data. (C) 2004 Elsevier Ltd. All rights reserved.
引用
收藏
页码:2705 / 2709
页数:5
相关论文
共 18 条
[1]
LIMONOIDS OF CALAMONDIN SEEDS [J].
BENNETT, RD ;
HASEGAWA, S .
TETRAHEDRON, 1981, 37 (01) :17-24
[2]
CAMERON JAMES W., 1961, HILGARDIA, V30, P359
[4]
Purification of limonoid glucosyltransferase from navel orange albedo tissues [J].
Hasegawa, S ;
Suhayda, CG ;
Hsu, WJ ;
Robertson, GH .
PHYTOCHEMISTRY, 1997, 46 (01) :33-37
[5]
BIOSYNTHESIS OF LIMONOIDS - CONVERSION OF DEACETYLNOMILINATE TO NOMILIN IN CITRUS-LIMON [J].
HASEGAWA, S ;
HERMAN, Z .
PHYTOCHEMISTRY, 1986, 25 (11) :2523-2524
[6]
METABOLISM OF LIMONOIDS - NOMILIN TO NOMILINATE IN CITRUS-LIMON [J].
HASEGAWA, S ;
HERMAN, Z ;
OU, P .
PHYTOCHEMISTRY, 1986, 25 (02) :542-543
[7]
LIMONOID GLUCOSIDES IN CITRUS [J].
HASEGAWA, S ;
BENNETT, RD ;
HERMAN, Z ;
FONG, CH ;
OU, P .
PHYTOCHEMISTRY, 1989, 28 (06) :1717-1720
[8]
BIOSYNTHESIS OF LIMONOIDS IN CITRUS SEEDLINGS [J].
HASEGAWA, S ;
BENNETT, RD ;
MAIER, VP .
PHYTOCHEMISTRY, 1984, 23 (08) :1601-1603
[9]
BIOSYNTHESIS OF LIMONOIDS IN CITRUS - SITES AND TRANSLOCATION [J].
HASEGAWA, S ;
HERMAN, Z ;
ORME, E ;
OU, P .
PHYTOCHEMISTRY, 1986, 25 (12) :2783-2785
[10]
HASEGAWA S, 1996, MOD METHOD PLANT, V18, P59