Voltammetric determination of microparticles of some local anesthetics and antithusics immobilized on the graphite electrode

被引:41
作者
Komorsky-Lovric, S [1 ]
Vukasinovic, N [1 ]
Penovski, R [1 ]
机构
[1] Rudjer Boskovic Inst, Ctr Marine & Environm Res, Zagreb 10002, Croatia
关键词
benzocaine; cinchocaine; lidocaine; codeine; procaine; square-wave voltammetry; cyclic voltammetry;
D O I
10.1002/elan.200390067
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Solid microparticles of local anesthetics benzocaine, cinchocaine, lidocaine and procaine, and the antithusic codeine were mechanically immobilized on the surface of the paraffin impregnated graphite electrode and investigated by square-wave and cyclic voltammetry in order to develop a method for their qualitative determination. The measurements were performed in the pH range between 1 and 9. The square-wave frequency and amplitude were changed between 100 and 1000 Hz, and from 15 to 85 mV respectively. The scan rate in cyclic voltammetry was 1 V/s.
引用
收藏
页码:544 / 547
页数:4
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