From Al4B2O9 nanowires to Al18B4O33:Eu nanowires

被引:15
作者
Elssfah, Elawad [1 ]
Tang, Chengcun [1 ]
机构
[1] Cent China Normal Univ, Dept Phys, Wuhan 430079, Peoples R China
关键词
D O I
10.1021/jp070977r
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
In this paper we report on the synthesis of single-crystal Al4B2O9 nanowires by calcining the precursor powder made of disodium tetraborate decahydrate and aluminum nitride in air conditions. The as-received nanowires possess smooth surface with diameters varying between 20 and 50 nm. We can also obtain Al18B4O33:Eu nanowires with diameters varying between 50 and 70 nm by recalcining a mixture powder of the above obtained Al4B2O9 nanowires, K2SO4, and Eu2O3 in air. The structural and compositional characteristics of the as-synthesized products have been investigated by XRD, SEM, TEM, EDX, and SAED techniques. Photoluminescence investigations reveal that Al18B4O33:Eu nanowires display emission peaks at 590.0, 613.4, and 628.8 nm.
引用
收藏
页码:8176 / 8179
页数:4
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