Pure Shift 1H NMR: A Resolution of the Resolution Problem?

被引:202
作者
Aguilar, Juan A. [1 ]
Faulkner, Stephen [2 ]
Nilsson, Mathias [1 ]
Morris, Gareth A. [1 ]
机构
[1] Univ Manchester, Sch Chem, Manchester M13 9PL, Lancs, England
[2] Univ Oxford, Inorgan Chem Lab, Oxford OX1 3QR, England
基金
英国工程与自然科学研究理事会;
关键词
DOSY; NMR spectroscopy; pure shift NMR; structure elucidation; NMR-SPECTRA; PROTON NMR; HOMONUCLEAR; SPECTROSCOPY; ELIMINATION; SIGNALS;
D O I
10.1002/anie.201001107
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
(Figure Presented)1H NMRspectra offers a large improvement in spectral resolution (see picture),equivalent to the use of a spectrometer in the GHz range. Such "pure shift" techniques are readily extended to multidimensional methods, for exmple DOSY. © 2010 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.
引用
收藏
页码:3901 / 3903
页数:3
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