Nanorod B phase VO2 obtained by using benzylamine as a reducing agent

被引:42
作者
Sediri, F.
Gharbi, N.
机构
[1] Univ Tunis, Lab Chim Mat Condensee, IPEITunis, Tunis, Tunisia
[2] Univ Tunis Elmanar, Fac Sci Tunis, Tunis, Tunisia
来源
MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY | 2007年 / 139卷 / 01期
关键词
vanadium dioxide; nanorods; benzylamine;
D O I
10.1016/j.mseb.2006.12.011
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Vanadium dioxide nanorod B phase with high purity and crystallinity was synthesized by using the crystalline V2O5 as precursor and benzylamine for the first time as reducing agent via hydrothermal method. The structure and morphology of the sample were characterized by scanning electron microscopy, transmission electron microscopy, X-ray powder diffraction, thermal analysis and infrared spectroscopy. Regularly sized nanorod B phase VO2 is about 20-100 nm wide and up to 2.5 mu m long. (c) 2006 Elsevier B.V. All rights reserved.
引用
收藏
页码:114 / 117
页数:4
相关论文
共 29 条
[1]  
Bieri F, 2001, HELV CHIM ACTA, V84, P3015, DOI 10.1002/1522-2675(20011017)84:10<3015::AID-HLCA3015>3.3.CO
[2]  
2-G
[3]   Synthesis of polyoxovanadates from aqueous solutions [J].
Bouhedja, L ;
Steunou, N ;
Maquet, J ;
Livage, J .
JOURNAL OF SOLID STATE CHEMISTRY, 2001, 162 (02) :315-321
[4]   Vanadium oxide: From gels to nanotubes [J].
Chandrappa, GT ;
Steunou, N ;
Cassaignon, S ;
Bauvais, C ;
Biswas, PK ;
Livage, J .
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2003, 26 (1-3) :593-596
[5]   Fabrication of novel vanadium dioxide nanorods as cathode material for rechargeable lithium batteries [J].
Chen, W ;
Peng, JF ;
Mai, LQ ;
Yu, H ;
Qi, YY .
CHEMISTRY LETTERS, 2004, 33 (10) :1366-1367
[6]   An ethylene glycol reduction approach to metastable VO2 nanowire arrays [J].
Chen, XY ;
Wang, X ;
Wang, ZH ;
Wan, JX ;
Liu, JW ;
Qian, YT .
NANOTECHNOLOGY, 2004, 15 (11) :1685-1687
[7]   Hydrothermal synthesis of vanadium oxides [J].
Chirayil, T ;
Zavalij, PY ;
Whittingham, MS .
CHEMISTRY OF MATERIALS, 1998, 10 (10) :2629-2640
[8]  
ERTL G, 1997, HDB HETEROGENOUS CAT, V4
[9]   Comparative study between nanocrystalline powder and thin film of vanadium dioxide VO2:: electrical and infrared properties [J].
Guinneton, F ;
Sauques, L ;
Valmalette, JC ;
Cros, F ;
Gavarri, JR .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2001, 62 (07) :1229-1238
[10]   SYNTHESIS OF VANADIUM DIOXIDE THIN-FILMS FROM VANADIUM ALKOXIDES [J].
GUZMAN, G ;
MORINEAU, R ;
LIVAGE, J .
MATERIALS RESEARCH BULLETIN, 1994, 29 (05) :509-515