Alcoholysis route to monodisperse CoO nanotetrapods with tunable size

被引:19
作者
Zhang, Yuliang
Zhong, Xinhua [1 ]
Zhu, Jian
Song, Xin
机构
[1] E China Univ Sci & Technol, Dept Chem, Adv Mat Lab, Shanghai 200237, Peoples R China
[2] Tongji Univ, Sch Life Sci & Technol, Shanghai 200092, Peoples R China
关键词
D O I
10.1088/0957-4484/18/19/195605
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Monodisperse tetrapod-shaped CoO nanocrystals were prepared via the alcoholysis of cobalt (III) oleate in dodecanol at high temperature. The coordinating solvent dodecanol also acts as a reducing and morphology controller reagent. The size of the obtained CoO nanotetrapods can be well tuned by variation of the amount of dodecanol used. The chemical composition, structure and morphology of the obtained nanocrystals were characterized by using energy-dispersive x-ray analysis, powder x-ray diffraction, and transmission electron microscopy.
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页数:5
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