Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion

被引：141

作者：

Crawford, D. E. ^{[1
]}

Wright, L. A. ^{[2
]}

James, S. L. ^{[1
]}

Abbott, A. P. ^{[2
]}

机构：

[1] Queens Univ Belfast, Sch Chem & Chem Engn, 39-123 Stranmillis Rd, Belfast BT9 5AG, Antrim, North Ireland

[2] Univ Leicester, Dept Chem, Leicester LE1 7RH, Leics, England

来源：

CHEMICAL COMMUNICATIONS | 2016年 / 52卷 / 22期

基金：

英国工程与自然科学研究理事会;

关键词：

MEDIA;

D O I：

10.1039/c5cc09685e

中图分类号：

O6 [化学];

学科分类号：

070301 [无机化学];

摘要：

Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE). This gave products in higher purity and with Space Time Yields (STYs), four orders of magnitude greater than for batch methods.

引用

页码：4215 / 4218

页数：4

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