Extraction of sesamin from sesame oil using macroporous resin

被引:45
作者
Zhou, Jia-Chun [1 ]
Feng, Da-Wei [1 ]
Zheng, Guo-Sheng [1 ]
机构
[1] E China Univ Sci & Technol, Dept Food Sci & Technol, Coll Biotechnol, Shanghai 200237, Peoples R China
关键词
Sesamin; Macroporous resin; Extraction; Adsorption; Desorption; CHROMATOGRAPHY; PURIFICATION; ADSORPTION; LIGNANS; INDICUM; ACID; RATS;
D O I
10.1016/j.jfoodeng.2010.04.011
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Sesamin is drawing research attention, due to its effects on the various body regulators. Currently there are two methods employed to separate sesamin: solvent extraction and steam stripping, but both methods have disadvantages in large-scale manufacturing systems. An innovative method for sesamin extraction from sesame oil has been unveiled in this paper, which employs macroporous resin as an adsorbing surface. The final product, sesamin crystal, has been obtained by crystallization of the desorption product. The concentration of sesamin in the desorption product was 9.7%, nearly 20-fold greater than in the starting sesame oil. After further refining, the concentration of sesamin in the final crystalline product reaches 76%. The procedure described in this paper demonstrates that a high concentration of sesamin can be obtained by employing resin adsorption. (C) 2010 Elsevier Ltd. All rights reserved.
引用
收藏
页码:289 / 293
页数:5
相关论文
共 18 条
[1]  
FUKUDA Y, 1988, NIPPON SHOKUHIN KOGY, V35, P483
[2]   GENERAL TREATMENT AND CLASSIFICATION OF SOLUTE ADSORPTION-ISOTHERM .1. THEORETICAL [J].
GILES, CH ;
SMITH, D ;
HUITSON, A .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1974, 47 (03) :755-765
[3]   LIGNAN ANALYSIS IN SEED OILS FROM 4 SESAMUM SPECIES - COMPARISON OF DIFFERENT CHROMATOGRAPHIC METHODS [J].
KAMALELDIN, A ;
APPELQVIST, LA ;
YOUSIF, G .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1994, 71 (02) :141-147
[4]   Microsphere resin chromatography combined with microbial biotransformation for the separation and purification of salvianolic acid B in aqueous extract of roots of Salvia multiorrihza Bunge [J].
Kan, Shidong ;
Li, Ji'an ;
Huang, Weiyi ;
Shao, Lei ;
Chen, Daijie .
JOURNAL OF CHROMATOGRAPHY A, 2009, 1216 (18) :3881-3886
[5]   Recovery of narirutin by adsorption on a non-ionic polar resin from a water-extract of Citrus unshiu peels [J].
Kim, Mi-Ryung ;
Kim, Won-Chul ;
Lee, Do-Youn ;
Kim, Chan-Wha .
JOURNAL OF FOOD ENGINEERING, 2007, 78 (01) :27-32
[6]   Sesamin is one of the major precursors of mammalian lignans in sesame seed (Sesamum indicum) as observed in vitro and in rats [J].
Liu, Z ;
Saarinen, NM ;
Thompson, LU .
JOURNAL OF NUTRITION, 2006, 136 (04) :906-912
[7]  
Nakano D., 2004, VASC DIS PREV, V1, P233
[8]  
OMOHUNDRO AL, 1949, Patent No. 2467903
[9]   Seperation and purification of ferulic acid in alkaline-hydrolysate from sugarcane bagasse by activated charcoal adsorption/anion macroporous resin exchange chromatography [J].
Ou, Shiyi ;
Luo, Yanlin ;
Xue, Feng ;
Huang, Caihuan ;
Zhang, Ning ;
Liu, Zili .
JOURNAL OF FOOD ENGINEERING, 2007, 78 (04) :1298-1304
[10]  
OZAKI T, 1993, Patent No. 5209826