The cheletropic trapping of nitric oxide by the bis-ketene 1,2-dicarbonylcyclohexa-3,5-diene and the diene 3,4-diphenyl-2,5-dimethyl-2,4-hexadiene.

被引：11

作者：

Adam, W

Bottle, SE

Grice, ID

Pfeiler, D

Wentrup, C

机构：

[1] QUEENSLAND UNIV TECHNOL,SCH CHEM,CIDC,BRISBANE,QLD 4001,AUSTRALIA

[2] UNIV WURZBURG,INST ORGAN CHEM,D-97074 WURZBURG,GERMANY

[3] UNIV QUEENSLAND,DEPT CHEM,BRISBANE,QLD 4072,AUSTRALIA

来源：

TETRAHEDRON LETTERS | 1996年 / 37卷 / 12期

关键词：

D O I：

10.1016/0040-4039(96)00206-7

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

We report the first example of the cheletropic trapping of nitric oxide with a bis-ketene. In the presence of nitric oxide the bis-ketene 12-dicarbonylcyclohexa-3,5-diene (1), generated from photolysis of benzocyclobutenedione, gave N-hydroxyphthalimide (5) and phthalic anhydride (7); additionally, cheletropic NO trapping with 3,4-diphenyl-2,5-dimethyl-2,4-hexadiene (3) gave strong persistent ESR signals, the nature of which was dependent on the purity of the NO.

引用

页码：2113 / 2116

页数：4

共 17 条

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