Purity assessment of multiwalled carbon nanotubes by Raman spectroscopy

被引：432

作者：

DiLeo, Roberta A. ^{[1
]}

Landi, Brian J.

Raffaelle, Ryne P.

机构：

[1] Rochester Inst Technol, Dept Phys, Rochester, NY 14623 USA

[2] Rochester Inst Technol, NPRL, Rochester, NY 14623 USA

来源：

JOURNAL OF APPLIED PHYSICS | 2007年 / 101卷 / 06期

关键词：

Multiwalled carbon nanotubes (MWCN);

D O I：

10.1063/1.2712152

中图分类号：

O59 [应用物理学];

学科分类号：

摘要：

Carbonaceous purity assessment for chemical vapor deposition multiwalled carbon nanotubes (MWNTs) using Raman spectroscopy was investigated. Raman spectroscopy was performed on a reference sample set containing predetermined ratios of MWNTs and representative synthesis by-products. Changes in the characteristic Raman peak ratios (i.e., I-D/I-G, I-G(')/I-G, and I-G(')/I-D) as a function of MWNT content were measured. Calibration curves were generated from the reference samples and used to evaluate MWNTs synthesized under different conditions with varying purity. The efficacy of using Raman spectroscopy in conjunction with thermogravimetric analysis for quantitative MWNT purity assessment is discussed. (c) 2007 American Institute of Physics.

引用

页数：5

共 16 条

[11] High-yield, nondestructive purification and quantification method for multiwalled carbon nanotubes [J].

Murphy, R ;

Coleman, JN ;

Cadek, M ;

McCarthy, B ;

Bent, M ;

Drury, A ;

Barklie, RC ;

Blau, WJ .

JOURNAL OF PHYSICAL CHEMISTRY B, 2002, 106 (12) :3087-3091

[12] Carbon nanotubes for power applications [J].

Raffaelle, RP ;

Landi, BJ ;

Harris, JD ;

Bailey, SG ;

Hepp, AF .

MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2005, 116 (03) :233-243

[13] Double resonance Raman spectroscopy of single-wall carbon nanotubes -: art. no. 157 [J].

Saito, R ;

Grüneis, A ;

Samsonidze, GG ;

Brar, VW ;

Dresselhaus, G ;

Dresselhaus, MS ;

Jorio, A ;

Cançado, LG ;

Fantini, C ;

Pimenta, MA ;

Souza, AG .

NEW JOURNAL OF PHYSICS, 2003, 5 :157.1-157.15

[14]

XU Y, 2006, J APPL PHYS, V100, P1

[15] Optical properties of aligned carbon nanotube mats for photonic applications [J].

Zhao, G. L. ;

Bagayoko, D. ;

Yang, L. .

JOURNAL OF APPLIED PHYSICS, 2006, 99 (11)

[16] Characteristic Raman spectra of multiwalled carbon nanotubes [J].

Zhao, X ;

Ando, Y ;

Qin, LC ;

Kataura, H ;

Maniwa, Y ;

Saito, R .

PHYSICA B-CONDENSED MATTER, 2002, 323 (1-4) :265-266

← 1 2 →