In situ wide angle X-ray scattering (WAXS) study of bimetallic Au-Pd catalysts

被引:4
作者
Canton, P
Riello, P
Furlan, A
Minesso, A
Bertoldo, L
Pinna, F
Benedetti, A
机构
[1] Univ Venice, Dipartimento Chim Fis, I-30123 Venice, Italy
[2] Univ Venice, Dipartimento Chim, I-30123 Venice, Italy
关键词
X-ray diffraction; gold; palladium; bimetallic catalysts; metal alloy; microstructure; Rietveld method;
D O I
10.1023/A:1019080714240
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Aim of the paper is to apply a modified version of the Rietveld method to two Au-Pd/C catalysts prepared by successive impregnation and reduced in situ by a special holder in order to show that a suitable WAXS analysis, performed in routine lab and using an X-ray conventional generator, can be very detailed and rich of information especially when a bimetallic catalyst has to be considered.
引用
收藏
页码:17 / 20
页数:4
相关论文
共 7 条
[1]   ASAXS investigation of a Au/C catalyst [J].
Benedetti, A ;
Polizzi, S ;
Riello, P ;
Pinna, F ;
Goerigk, G .
JOURNAL OF CATALYSIS, 1997, 171 (01) :345-348
[2]   A PROFILE-FITTING PROCEDURE FOR ANALYSIS OF BROADENED X-RAY-DIFFRACTION PEAKS .2. APPLICATION AND DISCUSSION OF THE METHODOLOGY [J].
BENEDETTI, A ;
FAGHERAZZI, G ;
ENZO, S ;
BATTAGLIARIN, M .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1988, 21 :543-549
[3]   Catalysis by gold [J].
Bond, GC ;
Thompson, DT .
CATALYSIS REVIEWS-SCIENCE AND ENGINEERING, 1999, 41 (3-4) :319-388
[4]  
Lemaitre J. L., 1984, CHARACTERIZATION HET, P299
[5]   Characterization of silica-supported Pd-Au clusters by X-ray absorption spectroscopy [J].
Reifsnyder, SN ;
Lamb, HH .
JOURNAL OF PHYSICAL CHEMISTRY B, 1999, 103 (02) :321-329
[6]   Au/C catalyst: Experimental evidence of the coexistence of nanoclusters and larger Au particles [J].
Riello, P ;
Canton, P ;
Benedetti, A .
LANGMUIR, 1998, 14 (23) :6617-6619
[7]  
RIELLO P, IN PRESS STUD SURF A