Multiplex phase cycling

被引:42
作者
Ivchenko, N
Hughes, CE
Levitt, MH [1 ]
机构
[1] Univ Southampton, Dept Chem, Southampton SO17 1BJ, Hants, England
[2] Stockholm Univ, Div Phys Chem, S-10691 Stockholm, Sweden
关键词
phase cycling; coherence transfer pathways; multiplex phase cycles; pure-absorption phase;
D O I
10.1016/S1090-7807(02)00108-8
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
We discuss a new class of phase cycling procedures, in which a set of individual phase-shifted transients are stored separately in the computer and processed afterwards to yield the separated NMR signals from two or more coherence transfer pathways. In the case of two-dimensional double-quantum spectroscopy, this multiplex acquisition procedure allows the acquisition of pure-absorption spectra in only 62.5% of the time needed by previous methods. (C) 2002 Elsevier Science (USA). All rights reserved.
引用
收藏
页码:52 / 58
页数:7
相关论文
共 24 条
[1]   PHASE SEPARATION IN 2-DIMENSIONAL SPECTROSCOPY [J].
BACHMANN, P ;
AUE, WP ;
MULLER, L ;
ERNST, RR .
JOURNAL OF MAGNETIC RESONANCE, 1977, 28 (01) :29-39
[2]  
Bain A.D., 1984, J MAGN RESON, V56, P418
[3]   ASSIGNMENT OF C-13 NMR-SPECTRA VIA DOUBLE-QUANTUM COHERENCE [J].
BAX, A ;
FREEMAN, R ;
FRENKIEL, TA ;
LEVITT, MH .
JOURNAL OF MAGNETIC RESONANCE, 1981, 43 (03) :478-483
[4]   SELECTION OF COHERENCE-TRANSFER PATHWAYS IN NMR PULSE EXPERIMENTS [J].
BODENHAUSEN, G ;
KOGLER, H ;
ERNST, RR .
JOURNAL OF MAGNETIC RESONANCE, 1984, 58 (03) :370-388
[5]   Synchronous helical pulse sequences in magic-angle spinning nuclear magnetic resonance:: Double quantum recoupling of multiple-spin systems [J].
Brinkmann, A ;
Edén, M ;
Levitt, MH .
JOURNAL OF CHEMICAL PHYSICS, 2000, 112 (19) :8539-8554
[6]  
DROBNY G, 1979, FARADAY DIV CHEM SOC, V13, P49
[7]  
Ernst R. R., 1987, PRINCIPLES NUCL MAGN
[8]   ELIMINATION OF DISPERSION-MODE CONTRIBUTIONS FROM 2-DIMENSIONAL NMR-SPECTRA [J].
FREEMAN, R ;
KEMPSELL, SP ;
LEVITT, MH .
JOURNAL OF MAGNETIC RESONANCE, 1979, 34 (03) :663-667
[9]   ISOTROPIC SPECTRA OF HALF-INTEGER QUADRUPOLAR SPINS FROM BIDIMENSIONAL MAGIC-ANGLE-SPINNING NMR [J].
FRYDMAN, L ;
HARWOOD, JS .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1995, 117 (19) :5367-5368
[10]  
HAGEMEYER A, 1989, ADV MAGN RESON, V13, P85