Multiplex phase cycling

被引:42
作者
Ivchenko, N
Hughes, CE
Levitt, MH [1 ]
机构
[1] Univ Southampton, Dept Chem, Southampton SO17 1BJ, Hants, England
[2] Stockholm Univ, Div Phys Chem, S-10691 Stockholm, Sweden
关键词
phase cycling; coherence transfer pathways; multiplex phase cycles; pure-absorption phase;
D O I
10.1016/S1090-7807(02)00108-8
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
We discuss a new class of phase cycling procedures, in which a set of individual phase-shifted transients are stored separately in the computer and processed afterwards to yield the separated NMR signals from two or more coherence transfer pathways. In the case of two-dimensional double-quantum spectroscopy, this multiplex acquisition procedure allows the acquisition of pure-absorption spectra in only 62.5% of the time needed by previous methods. (C) 2002 Elsevier Science (USA). All rights reserved.
引用
收藏
页码:52 / 58
页数:7
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