Solid-phase extraction as a clean-up procedure for the liquid chromatographic determination of benzoic and sorbic acids in fruit-derived products

被引:10
作者
Mandrou, B [1 ]
Nolleau, V [1 ]
Gastaldi, E [1 ]
Fabre, H [1 ]
机构
[1] Fac Pharm Montpellier, Chim Analyt Lab, F-34060 Montpellier 2, France
关键词
D O I
10.1080/10826079808000512
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A liquid-chromatographic procedure is proposed for the simultaneous determination of benzoic and sorbic acids in fruit-derived products. Prior to the chromatographic separation, a clean-up pre-treatment of the sample is carried out off-line, using successively an anionic resin and a C-18 stationary phase as sorbent beds. After elution from the cartridges, the acids are separated and quantitated by LC with UV-absorbance detection. The validation tests show that the technique can be applied to different types of fruit-derived products (i.e. jams, dried fruits and almond paste).
引用
收藏
页码:829 / 842
页数:14
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