Versatile gas/liquid microreactors for industry

被引:29
作者
Chambers, RD
Fox, MA
Holling, D
Nakano, T
Okazoe, T
Sandford, G
机构
[1] Univ Durham, Dept Chem, Durham DH1 3LE, England
[2] Asahi Glass Co Ltd, Yokohama, Kanagawa 2218755, Japan
关键词
D O I
10.1002/ceat.200407123
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
The design, fabrication, use and scale-out of versatile, multi-channel gas/liquid microreactors, which are suitable for both laboratory and industrial syntheses, are described. Direct fluorination reactions of diethyl malonate and Meldrum's acid using the new microreactor technology were studied to demonstrate the viability of the device for carrying out gas/liquid processes, particularly when using potentially hazardous materials.
引用
收藏
页码:344 / 352
页数:9
相关论文
共 25 条
  • [1] [Anonymous], 1991, Fluorine in Bioorganic Chemistry
  • [2] Baasner B., 2000, HOUBEN WEYL ORGANOFL, VE10a
  • [3] Banks R.E., 1994, ORGANOFLUORINE CHEM
  • [4] Chambers R. D., 2002, [No title captured], Patent No. [PCT/GB03/01993, 0301993]
  • [5] Chambers RD, 2004, CHIM OGGI, V22, P6
  • [6] Elemental fluorine - Part 16. Versatile thin-film gas-liquid multi-channel microreactors for effective scale-out
    Chambers, RD
    Fox, MA
    Holling, D
    Nakano, T
    Okazoe, T
    Sandford, G
    [J]. LAB ON A CHIP, 2005, 5 (02) : 191 - 198
  • [7] Elemental fluorine - Part 13. Gas-liquid thin film microreactors for selective direct fluorination
    Chambers, RD
    Holling, D
    Spink, RCH
    Sandford, G
    [J]. LAB ON A CHIP, 2001, 1 (02): : 132 - 137
  • [8] Elemental fluorine .3. The preparation of dialkyl fluoromalonates by direct fluorination
    Chambers, RD
    Hutchinson, J
    Thomson, J
    [J]. JOURNAL OF FLUORINE CHEMISTRY, 1996, 78 (02) : 165 - 166
  • [9] Elemental fluorine. Part 9 - Catalysis of the direct fluorination of 2-substituted carbonyl compounds
    Chambers, RD
    Hutchinson, J
    [J]. JOURNAL OF FLUORINE CHEMISTRY, 1998, 92 (01) : 45 - 52
  • [10] Microreactors for elemental fluorine
    Chambers, RD
    Spink, RCH
    [J]. CHEMICAL COMMUNICATIONS, 1999, (10) : 883 - 884