Determination of the trace 1,4-dioxane

被引：17

作者：

Guo, WQ ^{[1
]}

Brodowsky, H

机构：

[1] Zhejiang Univ, Dept Chem, Hangzhou 310028, Peoples R China

[2] Univ Kiel, Inst Phys Chem, D-24118 Kiel, Germany

来源：

MICROCHEMICAL JOURNAL | 2000年 / 64卷 / 02期

关键词：

1,4-dioxane; thermal desorption; neural network; gas chromatography;

D O I：

10.1016/S0026-265X(99)00026-0

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A simple, fast and sensitive new method for the determination of 1,4-dioxane traces in food additives is reported. The matrix effect and column contamination was reduced by means of using thermal desorption-gas chromatography with a submicro-particle packed column. The chromatographic conditions were optimized by means of two methods - orthogonal test and artificial neural networks (ANN). The detection limit was 0.05 similar to 0.10 mg/kg, the linear range was large, and the correlation coefficient was 0.99. The method is suitable for quality control in food production and surveillance. (C) 2000 Elsevier Science B.V. All rights reserved.

引用

页码：173 / 179

页数：7