A facile one-pot method for the preparation of N-alkyl isatins under microwave irradiation

被引：24

作者：

Azizian, J

Fallah-Bagher-Shaidaei, H

Kefayati, H

机构：

[1] Shaheed Beheshti Univ, Dept Chem, Tehran, Iran

[2] Islamic Azad Univ, Dept Chem, Rasht, Iran

[3] Islamic Azad Univ, Dept Chem, Tehran, Iran

来源：

SYNTHETIC COMMUNICATIONS | 2003年 / 33卷 / 05期

关键词：

D O I：

10.1081/SCC-120016324

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

N-Alkyl isatins have been prepared by reaction of the isatin and 5-bromoisatin with K(2)CO(3) and convenient alkyl halides in DMF under microwave irradiation with the high yield, simple work-up and short time.

引用

页码：789 / 793

页数：5

共 10 条

[1] CINNOLINES .9. STOLLE-BECKER SYNTHESIS
BAUMGARTEL, H
FURNAS, JL
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1961, 26 (05) : 1536 - &
[2] STEREOCONTROL OF BETA-LACTAM FORMATION USING MICROWAVE IRRADIATION
BOSE, AK
BANIK, BK
MANHAS, MS
[J]. TETRAHEDRON LETTERS, 1995, 36 (02) : 213 - 216
[3] MICROWAVE-ASSISTED ORGANIC-REACTIONS
CADDICK, S
[J]. TETRAHEDRON, 1995, 51 (38) : 10403 - 10432
[4] GENERAL METHOD FOR SYNTHESIS OF ISATINS
GASSMAN, PG
CUE, BW
LUH, TY
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1977, 42 (08) : 1344 - 1348
[5] KOHAN M, 1913, MONTASH CHEM, V34, P787
[6] Majumdar KC, 1996, J CHEM RES-S, P460
[7] MORICONI EJ, 1964, J ORG CHEM, P3577
[8] RADUL OM, 1980, KHIM GETEROTSIKL, V11, P1562
[9] SETTIMO AD, 1970, J ORG CHEM, V35, P2546
[10] CLAY CATALYSIS - DRY CONDENSATION OF 3-METHYL-1-PHENYL-5-PYRAZOLONE WITH ALDEHYDES UNDER MICROWAVE IRRADIATION
VILLEMIN, D
LABIAD, B
[J]. SYNTHETIC COMMUNICATIONS, 1990, 20 (20) : 3213 - 3218

← 1 →