Morphology control of MnWO4 nanocrystals by a solvothermal route

被引:52
作者
Chen, SJ
Chen, XT [1 ]
Xue, ZL
Zhou, JH
Li, J
Hong, JM
You, XZ
机构
[1] State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China
[2] Inst Coordinat Chem, Nanjing 210093, Peoples R China
[3] Univ Tennessee, Dept Chem, Knoxville, TN 37996 USA
[4] Nanjing Univ, Analyt Ctr, Nanjing, Peoples R China
关键词
D O I
10.1039/b300457k
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A solvothermal route to MnWO4 nanoparticles and nanorods has been developed. These nano-size products have been characterized by X-ray diffraction and transmission electron microscopy. The pressure, pH and temperature of the reaction systems were found to play important roles in determining the morphologies of the MnWO4 nanocrystalline products. Homologous surfactants have also been used to control the formation of MnWO4 nanocrystals. These surfactants were found to play a crucial role in the solvothermal route, and there is apparently a relationship between the molecular weight of the added homologous surfactants and the aspect ratio of the resulting nanorods.
引用
收藏
页码:1132 / 1135
页数:4
相关论文
共 19 条
[11]   Hydrothermal preparation and characterization of luminescent CdWO4 nanorods [J].
Liao, HW ;
Wang, YF ;
Liu, XM ;
Li, YD ;
Qian, YT .
CHEMISTRY OF MATERIALS, 2000, 12 (10) :2819-+
[12]  
Patzke GR, 2002, ANGEW CHEM INT EDIT, V41, P2446, DOI 10.1002/1521-3773(20020715)41:14<2446::AID-ANIE2446>3.0.CO
[13]  
2-K
[14]   Comparative study on micromorphology and humidity sensitive properties of thin-film and thick-film humidity sensors based on semiconducting MnWO4 [J].
Qu, WM ;
Wlodarski, W ;
Meyer, JU .
SENSORS AND ACTUATORS B-CHEMICAL, 2000, 64 (1-3) :76-82
[15]   ZUR CHEMIE IN SCHMELZLOSUNGEN .3. DARSTELLUNG KRISTALLINER WOLFRAMATE ME2+WO4 [J].
SCHULTZE, D ;
WILKE, KT ;
WALIGORA, C .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1967, 352 (3-4) :184-&
[16]   Molecular manipulation of microstructures: Biomaterials, ceramics, and semiconductors [J].
Stupp, SI ;
Braun, PV .
SCIENCE, 1997, 277 (5330) :1242-1248
[17]  
Sun JH, 2000, CHEM J CHINESE U, V21, P95
[18]   Size-controlled synthesis of magnetite nanoparticles [J].
Sun, SH ;
Zeng, H .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2002, 124 (28) :8204-8205
[19]   CERAMIC SENSORS FOR HUMIDITY DETECTION - THE STATE-OF-THE-ART AND FUTURE-DEVELOPMENTS [J].
TRAVERSA, E .
SENSORS AND ACTUATORS B-CHEMICAL, 1995, 23 (2-3) :135-156