Determination of Lead, Iron, Manganese and Zinc in Sea Water Samples by Atomic Absorption Spectrometry after Preconcentration with Chromosorb 105

被引：15

作者：

Baga, Huseyin ^{[1
]}

Elci, Aydan ^{[2
]}

Elci, Latif ^{[3
]}

机构：

[1] Pamukkale Univ, Fac Educ, Dept Sci Educ, TR-20020 Denizli, Turkey

[2] Ege Univ, Fac Sci, Dept Chem, TR-35100 Izmir, Turkey

[3] Pamukkale Univ, Fac Sci & Arts, Dept Chem, TR-20017 Denizli, Turkey

来源：

EURASIAN JOURNAL OF ANALYTICAL CHEMISTRY | 2006年 / 1卷 / 01期

关键词：

Preconcentration; Chromosorb; 105; Lead; Iron; Manganese; Zinc; Solid Phase Extraction; Atomic Absorption Spectrometry;

D O I：

10.12973/ejac.2006.00005a

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A solid phase extraction procedure based a column technique for preconcentration of lead, iron, manganese and zinc from water samples was developed. The analyte ions as its diethyldithiocarbamate complex were retained on a column of Chromosorb 105 from buffered sample solution. Then they were eluted with acetone. The recoveries of lead, iron, manganese and zinc under the optimum working conditions were 100, 97, 100 and 100%, respectively. The relative standard deviations were less than 6%. The method presented was applied for the determination of lead, iron, zinc and manganese in sea water samples.

引用

页码：42 / 54

页数：13

共 45 条

[1] Solid phase extraction of some metal ions on Diaion-20 resin prior to flame atomic absorption spectrometric analysis [J].

Armagan, F ;

Soylak, M ;

Elci, L ;

Dogan, M .

JOURNAL OF TRACE AND MICROPROBE TECHNIQUES, 2002, 20 (01) :15-27

[2] Determination of trace metals in geological samples by atomic absorption spectrophotometry after preconcentration by Aspergillus niger immobilized on sepiolite [J].

Bag, H ;

Türker, AR ;

Lale, M .

ANALYTICAL SCIENCES, 1999, 15 (12) :1251-1256

[3] Determination of Cu, Zn, Fe, Ni and Cd by flame atomic absorption spectrophotometry after preconcentration by Escherichia coli immobilized on sepiolite [J].

Bag, H ;

Türker, AR ;

Lale, M .

TALANTA, 2000, 51 (05) :1035-1043

[4] Determination of iron and nickel by flame atomic absorption spectrophotometry after preconcentration on Saccharomyces cerevisiae immobilized sepiolite [J].

Bag, H ;

Lale, M ;

Turker, AR .

TALANTA, 1998, 47 (03) :689-696

[5] Determination of Cu, Zn and Cd in water by FAAS after preconcentration by baker's yeast (Saccharomyces cerevisiae) immobilized on sepiolite [J].

Bag, H ;

Lale, M ;

Türker, AR .

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1999, 363 (03) :224-230

[6] Determination of Fe(II) and Fe(III) in water by flame atomic absorption spectrophotometry after their separation with Aspergillus niger immobilized on sepiolite [J].

Bag, H ;

Türker, AR ;

Tunçeli, A ;

Lale, M .

ANALYTICAL SCIENCES, 2001, 17 (07) :901-904

[7] Determination of lead and nickel in environmental samples by flame atomic absorption spectrometry after column solid-phase extraction on Ambersorb-572 with EDTA [J].

Baytak, S ;

Türker, AR .

JOURNAL OF HAZARDOUS MATERIALS, 2006, 129 (1-3) :130-136

[8] Determination of iron(III), cobalt(II) and chromium(III) in various water samples by flame atomic absorption spectrometry after preconcentration by means of Saccharomyces carlsbergensis immobilized on amberlite XAD-4 [J].

Baytak, S ;

Türker, AR .

MICROCHIMICA ACTA, 2005, 149 (1-2) :109-116

[9]

Baytak S, 2004, TURK J CHEM, V28, P243

[10]

Cai Y, 2002, ATOM SPECTROSC, V23, P52

← 1 2 3 4 5 →