A SCANNING TUNNELING MICROSCOPE THAT OPERATES AT HIGH-PRESSURES AND HIGH-TEMPERATURES (430-K) AND DURING CATALYTIC REACTIONS

被引：59

作者：

MCINTYRE, BJ ^{[1
]}

SALMERON, MB ^{[1
]}

SOMORJAI, GA ^{[1
]}

机构：

[1] UNIV CALIF BERKELEY,DEPT CHEM,BERKELEY,CA 94720

来源：

CATALYSIS LETTERS | 1992年 / 14卷 / 3-4期

关键词：

SCANNING TUNNELING MICROSCOPY; STM; INSITU; PLATINUM;

D O I：

10.1007/BF00769663

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

We describe the construction and operation of a scanning tunneling microscope (STM) designed in our laboratory that is contained in a reaction cell and allows operation throughout a wide range of pressures (ultra-high vacuum-atmospheric) and temperatures (300-425 K). This thermally compensated, double piezo tube design is entirely mechanically clamped. Samples are inertially translated and can be easily transferred in and out of the STM. With this microscope, we have investigated the stability of Pt(110) as a function of oxygen and hydrogen pressure and temperature.

引用

页码：263 / 269

页数：7

共 7 条

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MERRILL, RP
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[2] THE PREPARATION, THERMAL-STABILITY AND ADSORPTION CHARACTERISTICS OF THE NON-RECONSTRUCTED PT(110)-1X1 SURFACE
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BONZEL, HP
[J]. SURFACE SCIENCE, 1982, 119 (2-3) : 234 - 250
[3] FROHN, 1989, PRAKT MET, V26, P518
[4] SURFACE PHASE-TRANSITIONS IN CO CHEMISORPTION ON PT(110)
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[5] DESIGN AND OPERATION OF A VARIABLE TEMPERATURE SCANNING TUNNELLING MICROSCOPE
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[6] LEED-AES STUDY OF THE RECONSTRUCTED PT(110) SURFACE AND THE EFFECT OF OXYGEN TREATMENT
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SOMORJAI, GA
[J]. SURFACE SCIENCE, 1980, 91 (2-3) : 373 - 384
[7] AN ULTRAHIGH-VACUUM SCANNING TUNNELING MICROSCOPE FOR SURFACE SCIENCE STUDIES
ZEGLINSKI, DM
OGLETREE, DF
BEEBE, TP
HWANG, RQ
SOMORJAI, GA
SALMERON, MB
[J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1990, 61 (12) : 3769 - 3774

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