学术探索
学术期刊
新闻热点
数据分析
智能评审

STUDY OF A NICKEL-CATALYZED GLASSY-CARBON ELECTRODE FOR DETECTION OF CARBOHYDRATES IN LIQUID-CHROMATOGRAPHY AND FLOW-INJECTION ANALYSIS

被引：77
作者：
CASELLA, IG
DEIMONI, F
CATALDI, TRI
机构：
[1] Dipartimento di Chimica, Università della Basilicata, Potenza
来源：
ANALYTICA CHIMICA ACTA | 1991年 / 248卷 / 01期
关键词：
LIQUID CHROMATOGRAPHY; FLOW SYSTEM; CYCLIC VOLTAMMETRY; AMPEROMETRY; CARBOHYDRATES;
D O I：
10.1016/S0003-2670(00)80876-4
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A nickel-modified glassy carbon electrode was investigated. The nickel deposit was characterized by electrochemical techniques, x-ray photoelectron spectroscopy and scanning electron microscopy. The described electrode was tested as detector in liquid chromatography and flow-injection analysis and showed a promising combination of background current stability, catalytic activity, detection limits and reproducibility for the determination of carbohydrates in real samples.
引用
收藏
页码：117 / 125
页数：9
相关论文
共 31 条
  • [1] BIOSENSING WITH COATED-WIRE ELECTRODES .1. GLUCOSE SENSORS
    ABDULLA, HM
    GREENWAY, GM
    PLATT, AE
    FIELDEN, PR
    [J]. ANALYST, 1989, 114 (07) : 785 - 788
  • [2] EFFECT OF PRE-TREATMENT OF PLATINUM FOR MODIFIED PLATINUM WIRE GLUCOSE-OXIDASE AMPEROMETRIC ELECTRODES
    BEH, SK
    MOODY, GJ
    THOMAS, JDR
    [J]. ANALYST, 1989, 114 (01) : 29 - 32
  • [3] PULSED AMPEROMETRIC DETECTION OF GLUCOSE IN BIOLOGICAL-FLUIDS AT A SURFACE-MODIFIED GOLD ELECTRODE
    BINDRA, DS
    WILSON, GS
    [J]. ANALYTICAL CHEMISTRY, 1989, 61 (22) : 2566 - 2570
  • [4] CASELLA IG, 1991, ANAL CHIM ACTA, V243, P61, DOI 10.1016/S0003-2670(00)82541-6
  • [5] COMBINATION ANALYSIS OF METAL-OXIDES USING ESCA, AES, AND SIMS
    CONNER, GR
    [J]. JOURNAL OF VACUUM SCIENCE & TECHNOLOGY, 1978, 15 (02): : 343 - 347
  • [6] Desimoni E., 1986, Computer Enhanced Spectroscopy, V3, P107
  • [7] DESIMONI E, IN PRESS J ELECTRON
  • [8] XPS STUDY OF COPPER ALUMINATE CATALYSTS
    ERTL, G
    HIERL, R
    KNOZINGER, H
    THIELE, N
    URBACH, HP
    [J]. APPLIED SURFACE SCIENCE, 1980, 5 (01) : 49 - 64
  • [9] FLEISCHMANN M, 1971, J ELECTROANAL CHEM, V31, P39, DOI 10.1016/0368-1874(71)80005-9
  • [10] X-RAY PHOTOEMISSION-STUDIES OF ATOM IMPLANTED MATRICES - NI IN CARBON
    GIBBS, RA
    WINOGRAD, N
    YOUNG, VY
    [J]. JOURNAL OF CHEMICAL PHYSICS, 1980, 72 (09) : 4799 - 4804
1234