AUTOMATIC PREPARATION OF MILK DESSERT SLURRIES FOR THE DETERMINATION OF TRACE AMOUNTS OF ALUMINUM BY ELECTROTHERMAL ATOMIC-ABSORPTION SPECTROMETRY

被引:23
作者
ARRUDA, MAZ [1 ]
GALLEGO, M [1 ]
VALCARCEL, M [1 ]
机构
[1] NATL UNIV CORDOBA, FAC SCI,DEPT ANALYT CHEM, E-14004 CORDOBA, SPAIN
关键词
ALUMINUM DETERMINATION; MILK DESSERT ANALYSES; ELECTROTHERMAL ATOMIC ABSORPTION SPECTROMETRY; SLURRY SAMPLE INTRODUCTION; FLOW INJECTION;
D O I
10.1039/ja9951000055
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method for the direct determination of aluminium in milk desserts is proposed, The method uses a how injection system connected semi-an-line to a graphite furnace atomic absorption spectrometer through an autosampler for preparation of the slurries, addition of a chemical modifier and dilution-homogenization in a mixing chamber. Calibration is performed with aqueous standards. The bow system can be used to implement the standard additions method and investigate the effect of potential interferents in parallel by using two injection loops and the merging-zones mode. The slurries prepared contained up to 10% m/v. Aluminium was determined in various milk desserts at concentrations between 0.007 and 0.121 mg per 100 g.
引用
收藏
页码:55 / 59
页数:5
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