A STRAIGHTFORWARD APPROACH TO THE SYNTHESIS OF UNSYMMETRICAL TETRATHIOALKYL TETRATHIAFULVALENE DERIVATIVES

被引：30

作者：

GEMMELL, C

KILBURN, JD

UECK, H

UNDERHILL, AE

机构：

[1] UNIV SOUTHAMPTON,DEPT CHEM,SOUTHAMPTON SO9 5NH,HANTS,ENGLAND

[2] UNIV WALES,DEPT CHEM,BANGOR LL57 2UW,GWYNEDD,WALES

来源：

TETRAHEDRON LETTERS | 1992年 / 33卷 / 27期

关键词：

D O I：

10.1016/S0040-4039(00)74820-9

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The p-acetoxybenzylthio protecting group has been found to be compatible with the triethylphosphite mediated cross-coupling of 4,5-dialkylthio-1,3-dithiol-2-ones, providing access to the tetrathiolate 5, and to dithiolates 11a and 11b, which are excellent precursors for unsymmetrical tetrathioalkyl tetrathiafulvalene derivatives.

引用

页码：3923 / 3926

页数：4

共 19 条

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