AN EFFECTIVE AND SELECTIVE SYNTHESIS OF STERICALLY CROWDED BENZOTRITHIOLES FROM BENZODITHIASTANNOLES VIA BENZOTRITHIOLE 2-OXIDES

被引：34

作者：

OGAWA, S ^{[1
]}

YOMOJI, N ^{[1
]}

CHIDA, S ^{[1
]}

SATO, R ^{[1
]}

机构：

[1] IWATE UNIV, FAC ENGN, DEPT APPL CHEM & MOLEC SCI, MORIOKA, IWATE 020, JAPAN

来源：

CHEMISTRY LETTERS | 1994年 / 03期

关键词：

D O I：

10.1246/cl.1994.507

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Sterically crowded benzotrithioles were efficiently and selectively prepared by the reduction of corresponding benzotrithiole 2-oxides which were readily obtained on treatment of benzodithiastannoles, synthetic equivalents of benzenedithiols, with thionyl chloride.

引用

页码：507 / 510

页数：4

共 28 条

[21] SULFUR-COMPOUNDS .144. SYNTHESIS OF SULFUR-RICH ORGANIC POLYSULFANES UTILIZING TITANOCENE PENTASULFIDE AS A SULFUR-TRANSFER REAGENT [J].

STEUDEL, R ;

FORSTER, S ;

ALBERTSEN, J .

CHEMISCHE BERICHTE, 1991, 124 (10) :2357-2359

[22] REDUCTION OF ALKYL ARYL SULFOXIDES BY IODIDE IONS IN ACID SOLUTION [J].

STRECKER, RA ;

ANDERSEN, KK .

JOURNAL OF ORGANIC CHEMISTRY, 1968, 33 (06) :2234-&

[23] 1,2,3-TRITHIOLE, 1,2,3-TRISELENOLE, AND 1,2,5-THIADISELENOLE - NOVEL RING-SYSTEMS DERIVED FROM STERICALLY PROTECTED 1,2,3-SELENADIAZOLE [J].

TOKITOH, N ;

ISHIZUKA, H ;

ANDO, W .

CHEMISTRY LETTERS, 1988, (04) :657-660

[24] COMPETITIVE PHOTOCHEMICAL DECARCOGENATION OF 1,2,5-THIADISELENOLE [J].

TOKITOH, N ;

ISHIZUKA, H ;

YABE, A ;

ANDO, W .

TETRAHEDRON LETTERS, 1989, 30 (22) :2955-2958

[25] NOVEL REACTIONS OF 1,1,4,4-TETRAARYL-1,2,3-BUTATRIENES WITH ELEMENTAL SULFUR AND SELENIUM [J].

TOKITOH, N ;

HAYAKAWA, H ;

GOTO, M ;

ANDO, W .

TETRAHEDRON LETTERS, 1988, 29 (16) :1935-1938

[26] NOVEL FORMATION AND MOLECULAR-STRUCTURE OF 1,2,3,4,5,6,7,8,9-NONATHIACYCLOUNDEC-10-ENE [J].

TOKITOH, N ;

OKANO, Y ;

ANDO, W ;

GOTO, M ;

MAKI, H .

TETRAHEDRON LETTERS, 1990, 31 (37) :5323-5326

[27] 1,2,3,4,5,6,7,8-OCTATHIONANE, A NOVEL CYCLIC POLYSULFIDE - SYNTHESIS AND CRYSTAL-STRUCTURE [J].

TOKITOH, N ;

TAKEDA, N ;

IMAKUBO, T ;

GOTO, M ;

OKAZAKI, R .

CHEMISTRY LETTERS, 1992, (08) :1599-1602

[28] OXIDATION OF BENZOTRITHIOLE ANALOGS - PHOTOCHEMICAL-REARRANGEMENT OF BENZOTRITHIOLE 2-OXIDES TO BENZOTRITHIOLE 1-OXIDES INVOLVING INTRAMOLECULAR OXYGEN MIGRATION [J].

YOMOJI, N ;

TAKAHASHI, S ;

CHIDA, S ;

OGAWA, S ;

SATO, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1993, (17) :1995-2000

← 1 2 3 →