A CONVENIENT AND IMPROVED PREPARATION OF CYANO-PHOSPHATES

被引：15

作者：

MICO, I ^{[1
]}

NAJERA, C ^{[1
]}

机构：

[1] UNIV ALICANTE,DEPT QUIM ORGAN,APDO 99,E-03080 ALICANTE,SPAIN

来源：

TETRAHEDRON | 1993年 / 49卷 / 20期

关键词：

D O I：

10.1016/S0040-4020(01)85749-5

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Cyano phosphates derived from aldehydes or ketones are prepared in good yields using lithium cyanide in DMF and diethyl chlorophosphate as phosphorylating agent.

引用

页码：4327 / 4332

页数：6

共 12 条

[1]

HARUSAWA S, 1983, CHEM PHARM BULL, V31, P2932

[2] NEW METHODS AND REAGENTS IN ORGANIC-SYNTHESIS .39. A NOVEL SYNTHESIS OF ALPHA,BETA-UNSATURATED NITRILES FROM AROMATIC KETONES VIA CYANOPHOSPHATES [J].

HARUSAWA, S ;

YONEDA, R ;

KURIHARA, T ;

HAMADA, Y ;

SHIOIRI, T .

TETRAHEDRON LETTERS, 1984, 25 (04) :427-428

[3]

KURIHARA T, 1986, CHEM PHARM BULL, V34, P4545

[4] APPLICATION OF CYANOHYDRIN O-DIETHYL PHOSPHATES IN ORGANIC-SYNTHESIS [J].

KURIHARA, T ;

HARUSAWA, S ;

YONEDA, R .

JOURNAL OF SYNTHETIC ORGANIC CHEMISTRY JAPAN, 1988, 46 (12) :1164-1178

[5]

KURIHARA T, 1986, CHEM PHARM BULL, V34, P4620

[6] REGIOSPECIFIC ARYLATION OF 1,4-BENZOQUINONE CYANOHYDRIN PHOSPHATE - SYNTHESIS OF 3-ARYL-4-HYDROXYBENZONITRILES [J].

KURIHARA, T ;

HARUSAWA, S ;

HIRAI, J ;

YONEDA, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1987, (08) :1771-1776

[7]

KURIHARA T, 1987, CHEM PHARM BULL, V35, P4777

[8]

KURIHARA T, 1986, CHEM PHARM BULL, V34, P2747

[9] A NEW SYNTHESIS OF POLYSUBSTITUTED CYCLOPROPANES [J].

YONEDA, R ;

SANTO, K ;

HARUSAWA, S ;

KURIHARA, T .

SYNTHETIC COMMUNICATIONS, 1987, 17 (08) :921-927

[10] DEPHOSPHORYLATION OF CYANO DIETHYL PHOSPHATES BY REDUCTION WITH LITHIUM LIQUID-AMMONIA - AN EFFICIENT METHOD FOR CONVERSION OF CARBONYL-COMPOUNDS INTO NITRILES [J].

YONEDA, R ;

OSAKI, T ;

HARUSAWA, S ;

KURIHARA, T .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1990, (03) :607-610

← 1 2 →