REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC SEPARATION OF TERTIARY AND QUATERNARY ALKALOIDS FROM CHELIDONIUM-MAJUS L

被引：23

作者：

HAN, LF ^{[1
]}

NOWICKY, W ^{[1
]}

GUTMANN, V ^{[1
]}

机构：

[1] VIENNA TECH UNIV,INST INORGAN CHEM,GETREIDEMARKT 9,A-1060 VIENNA,AUSTRIA

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 543卷 / 01期

关键词：

D O I：

10.1016/S0021-9673(01)95760-7

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A reversed-phase high-performance liquid chromatographic procedure is described for the determination of the alkaloids in Chelidonium majus L. extracts. For the analysis of tertiary and quaternary alkaloids, replacement of the commonly applied organic amine modifiers with potassium iodide led to a considerable improvement in resolution. By using a gradient elution programme more than twenty peaks were resolved and thirteen tertiary and quaternary alkaloids were identified.

引用

页码：123 / 128

页数：6

共 14 条

[11] PEAK TAILING AND RETENTION BEHAVIOR OF TRICYCLIC ANTI-DEPRESSANT AMINES AND RELATED HYDROPHOBIC AMMONIUM-COMPOUNDS IN REVERSED-PHASE ION-PAIR LIQUID-CHROMATOGRAPHY ON ALKYL-BONDED PHASES [J].

SOKOLOWSKI, A ;

WAHLUND, KG .

JOURNAL OF CHROMATOGRAPHY, 1980, 189 (03) :299-316

[12]

SPATH E, 1931, CHEM BER, V64, P1127

[13] QUANTITATIVE-ANALYSIS OF D-TUBOCURARINE CHLORIDE IN CURARE BY COLUMN LIQUID-CHROMATOGRAPHY [J].

VANDERMAEDEN, FPB ;

VANRENS, PT ;

BUYTENHUYS, FA ;

BUURMAN, E .

JOURNAL OF CHROMATOGRAPHY, 1977, 142 (NOV) :715-723

[14] REVERSED-PHASE ION-PAIR CHROMATOGRAPHY OF ANTIDEPRESSIVE AND NEUROLEPTIC AMINES AND RELATED QUATERNARY AMMONIUM-COMPOUNDS [J].

WAHLUND, KG ;

SOKOLOWSKI, A .

JOURNAL OF CHROMATOGRAPHY, 1978, 151 (03) :299-310

← 1 2 →