FLOW-INJECTION DETERMINATION OF HMF IN HONEY BY THE WINKLER METHOD

被引:18
作者
SALINAS, F [1 ]
MANSILLA, AE [1 ]
NEVADO, JJB [1 ]
机构
[1] UNIV CASTILLA LA MANCHA,DEPT CHEM,E-13071 CIUDAD REAL,SPAIN
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1991年 / 340卷 / 04期
关键词
D O I
10.1007/BF00321778
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new method for the semiautomatic determination of 5-hydroxymethylfurfural (HMF) by photometric flow injection analysis on the basis of the Winkler's reaction is proposed. The derivative FIA-gram signals were also obtained and detection limit was decreased. The linear range of determination is 2.3-98-mu-g.ml-1. The presence of sugars is well tolerated. The proposed method can be employed to determine HMF in honey samples with a sampling frequency of 35 h-1.
引用
收藏
页码:250 / 252
页数:3
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