ONE-POT SYNTHESIS OF 1,2-O-ISOPROPYLIDENE-ALPHA-D-XYLOFURANOSE

被引：79

作者：

MORAVCOVA, J

CAPKOVA, J

STANEK, J

机构：

[1] Department of Chemistry of Natural Compounds, Institute of Chemical Technology

来源：

CARBOHYDRATE RESEARCH | 1994年 / 263卷 / 01期

关键词：

1,2-O-ISOPROPYLIDENE-ALPHA-D-XYLOFURANOSE 1,2/3,5-DI-O-ISOPROPYLIDENE-ALPHA-D-XYLOFURANOSE; ACETALATION; D-XYLOSE; PARTIAL HYDROLYSIS;

D O I：

10.1016/0008-6215(94)00165-0

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

The title compound 1 was prepared by sulfuric acid-catalyzed acetalation of D-xylose followed by partial hydrolysis with aqueous sodium carbonate added directly to a crude acetalation mixture. The yield of crystalline 1 (mp 42-43 degrees C) was 80%.

引用

页码：61 / 66

页数：6