A RAPID AND TIME-EFFECTIVE ASSAY FOR DETERMINATION OF OXOLINIC ACID AND FLUMEQUINE IN FISH-TISSUES BY HPLC

被引:17
作者
HORMAZABAL, V
YNDESTAD, M
机构
[1] Division of Food Hygiene, Norwegian College of Veterinaty Medicine, N-0033, Oslo 1
来源
JOURNAL OF LIQUID CHROMATOGRAPHY | 1994年 / 17卷 / 13期
关键词
D O I
10.1080/10826079408013509
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A simple method for analysis of oxolinic acid and flumequine in fish muscle and liver is described. The samples were extracted with trichloroacetic acid, neutralized and analysed by HPLC, with minimal sample manipulation. The limit of quantification was 30 mu g/kg for oxolinic acid and 35 mu g/kg for flumequine. The simplified extraction and clean-up procedure makes it possible for one person to monitor the concentration of the drugs in approximately 80 samples per day.
引用
收藏
页码:2911 / 2917
页数:7
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