SYNTHESIS, SPECTROSCOPIC PROPERTIES AND MOLECULAR-STRUCTURE OF THE PARAMAGNETIC COMPLEX [(ETA(5)-3,5-DI-TERT-BUTYL-1,2,4-TRIPHOSPHACYCLOPENTADIENYL)(ETA(5)-2,4,5-TRI-TERT-BUTYL-1,3-DIPHOSPHACYCLOPENTADIENYL)]VANADIUM(II)

被引:25
作者
CLOKE, FGN
FLOWER, KR
HITCHCOCK, PB
NIXON, JF
机构
关键词
D O I
10.1039/c39950001659
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Cocondensation of vanadium vapour with the phosphaalkyne Bu(t)CP affords the paramagnetic complex [V(eta(5)-P(3)C(2)Bu(2)(t))(eta(5)-P(2)C(3)Bu(3)(t))], whose molecular structure is determined by a single crystal X-ray diffraction study.
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页码:1659 / 1660
页数:2
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共 21 条
  • [1] SYNTHESIS AND CHARACTERIZATION OF THE FIRST COMPOUNDS CONTAINING A STABLE PHOSPHIRENYL CATION - CRYSTAL-STRUCTURE AND MOLECULAR-STRUCTURE OF [NI(ETA(3)-PC(2)TBU(2))(ETA(5)-P(3)C(2)TBU(2))W(CO)(5)]
    AVENT, AG
    CLOKE, FGN
    FLOWER, KR
    HITCHCOCK, PB
    NIXON, JF
    VICKERS, DM
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1994, 33 (22): : 2330 - 2332
  • [2] HEXA-PHOSPHORUS ANALOGS OF METALLOCENES - SYNTHESIS OF THE 1ST PARAMAGNETIC SANDWICH COMPLEX CONTAINING 2 ETA-5-1,2,4-TRIPHOSPHACYCLOPENTADIENYL RINGS - CRYSTAL AND MOLECULAR-STRUCTURES OF [CR(ETA-5-C2(BU-TERT)2P3)2]
    BARTSCH, R
    HITCHCOCK, PB
    NIXON, JF
    [J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1988, 356 (01) : C1 - C4
  • [3] 1ST STRUCTURAL CHARACTERIZATION OF PENTA-PHOSPHORUS AND HEXA-PHOSPHORUS ANALOGS OF FERROCENE - SYNTHESIS, CRYSTAL AND MOLECULAR-STRUCTURE OF THE AIR-STABLE, SUBLIMABLE IRON SANDWICH COMPOUNDS [FE(ETA-5-C2BUT2P3)2], AND [FE(ETA-5-C3BUT3P2)(ETA-5-C2BUT2P3)]
    BARTSCH, R
    HITCHCOCK, PB
    NIXON, JF
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1987, (15) : 1146 - 1148
  • [4] 1,3,5,7-TETRAPHOSPHABARRELENE - A NEW CYCLIC PHOSPHAALKYNE TETRAMER
    BINGER, P
    GLASER, G
    GABOR, B
    MYNOTT, R
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1995, 34 (01): : 81 - 83
  • [5] PHOSPHORUS-COMPOUNDS OF UNUSUAL COORDINATION .11. 1,3-DIPHOSPHACYCLOBUTADIENECOBALT(I) COMPLEXES FROM PHOSPHAALKYNES
    BINGER, P
    MILCZAREK, R
    MYNOTT, R
    REGITZ, M
    ROSCH, W
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1986, 25 (07): : 644 - 645
  • [6] LAMBDA-3-1,3-DIPHOSPHACYCLOBUTADIENE-COBALT COMPLEXES BY CYCLO-DIMERIZATION OF LAMBDA-3-PHOSPHAALKYNES
    BINGER, P
    MILCZAREK, R
    MYNOTT, R
    KRUGER, C
    TSAY, YH
    RAABE, E
    REGITZ, M
    [J]. CHEMISCHE BERICHTE-RECUEIL, 1988, 121 (04): : 637 - 645
  • [7] SYNTHESIS AND MOLECULAR-STRUCTURE OF TRIS(ETA(4)-2,4-DI-TERT-BUTYL-1,3-DIPHOSPHACYCLOBUTADIENE)MOLYBDENUM(0)
    CLOKE, FGN
    FLOWER, KR
    HITCHCOCK, PB
    NIXON, JF
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1994, (04) : 489 - 490
  • [8] REACTIVE PI-COMPLEXES OF ELECTRON-RICH TRANSITION-METALS .4. CYCLIZATION REACTIONS OF TERT-BUTYLPHOSPHAACETYLENE WITH PI-ARENE-IRON COMPLEXES
    DRIESS, M
    HU, D
    PRITZKOW, H
    SCHAUFELE, H
    ZENNECK, U
    REGITZ, M
    ROSCH, W
    [J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1987, 334 (03) : C35 - C38
  • [9] EMSLEY J, 1989, ELEMENTS, P52
  • [10] THE DETERMINATION OF THE PARAMAGNETIC SUSCEPTIBILITY OF SUBSTANCES IN SOLUTION BY NUCLEAR MAGNETIC RESONANCE
    EVANS, DF
    [J]. JOURNAL OF THE CHEMICAL SOCIETY, 1959, (JUN): : 2003 - 2005