Near infrared diffuse reflectance spectrophotometry, within the wavelength range 1,100 to 2,500 nm, was investigated for use in the simultaneous prediction of the moisture, organic C, and total N contents of air-dried soils. An infraAlyzer 500 C (Technicon Instruments Corp. ) scanning spectrophotometer was used to obtain near infrared reflectance of soils at 2-nm intervals. Calibration equations for each of the soil constituents studied were based upon selection of the best combination of three wavelengths in a multiple regression analysis.