SYNTHESIS AND CHARACTERIZATION OF STATIONARY PHASES ON THE BASIS OF SILICAS MODIFIED WITH EPOXIDIZED POLYBUTADIENES .4. CHROMATOGRAPHIC EXPERIMENTS ON A NEW AMINO-FUNCTIONALIZED STATIONARY PHASE FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：8

作者：

ERLER, U

HEUBLEIN, G

机构：

[1] Department of Chemistry, Friedrich-Schiller-University of Jena, D-6900 Jena

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 588卷 / 1-2期

关键词：

D O I：

10.1016/0021-9673(91)85043-F

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Amino-functionalized stationary phases derived from polybutadiene epoxide-coated silica possess a good stability in aqueous buffer solutions at different pH. Pressure stability of the highly polymer-loaded support, separation of carbohydrates, purines and pyrimidines, and the influence of the pH of the eluent mixture on the retention behaviour of ionisable samples, such as substituted benzoic acids, are demonstrated.

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页码：340 / 343

页数：4

相关论文

共 15 条

[1] SYNTHESIS AND CHARACTERIZATION OF STATIONARY PHASES BASED ON POLYSILICIC ACIDS MODIFIED WITH EPOXIDIZED POLYBUTADIENE (PBDE) .3. STUDIES ON THE SYNTHESIS OF AMINE-FUNCTIONALIZED SEPARATION-MATERIALS AND CARRIER-MATERIALS [J].

ERLER, U ;

HEUBLEIN, G .

ANGEWANDTE MAKROMOLEKULARE CHEMIE, 1990, 182 :43-61

[2] SYNTHESIS AND CHARACTERIZATION OF STATIONARY PHASES ON THE BASIS OF SILICAS MODIFIED WITH EPOXIDIZED POLYBUTADIENES - SYNTHESIS AND CHARACTERIZATION OF A NEW POLYHYDROXY FUNCTIONALIZED STATIONARY PHASE FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY .1. [J].

ERLER, U ;

SPANGE, S ;

HEUBLEIN, G .

ACTA POLYMERICA, 1991, 42 (08) :389-393

[3] EFFECT OF COLUMN DEGRADATION ON THE REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC SEPARATION OF PEPTIDES AND PROTEINS [J].

GLAJCH, JL ;

KIRKLAND, JJ ;

KOHLER, J .

JOURNAL OF CHROMATOGRAPHY, 1987, 384 :81-90

[4]

HANAI T, 1986, ADV CHROMATOGR, V25, P280

[5] NEW POLYMER COATED ANION-EXCHANGE HPLC-PHASES - IMMOBILIZATION OF POLY (2-HYDROXY, 3N-ETHYLENEDIAMINO) BUTADIENE ON SILICA AND ALUMINA [J].

HEINEMANN, G ;

KOHLER, J ;

SCHOMBURG, G .

CHROMATOGRAPHIA, 1987, 23 (06) :435-441

[6] REACTION COMPOSITES FROM POLYFUNCTIONAL MACROMOLECULES AND INORGANIC SOLIDS [J].

HEUBLEIN, G ;

HEUBLEIN, B ;

HORTSCHANSKY, P ;

MEISSNER, H ;

SCHUTZ, H .

JOURNAL OF MACROMOLECULAR SCIENCE-CHEMISTRY, 1988, A25 (02) :183-200

[7] SYNTHESIS AND CHARACTERIZATION OF STATIONARY PHASES BASED ON POLYSILICIC ACIDS MODIFIED WITH EPOXIDIZED POLYBUTADIENE (PBDE) .1. STUDIES ON THE SURFACE MODIFICATION OF POLYSILICIC ACIDS WITH EPOXIDIZED POLYBUTADIENES [J].

HEUBLEIN, G ;

ERLER, U ;

ULBRICHT, A ;

WINKELMANN, H .

ANGEWANDTE MAKROMOLEKULARE CHEMIE, 1990, 182 :29-42

[8]

HEUBLEIN G, 1989, MAKROMOL CHEM, V190, P9

[9] LIQUID-CHROMATOGRAPHY APPLIED TO OLIGOSACCHARIDE FRACTIONATION [J].

HEYRAUD, A ;

RINAUDO, M .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1981, 4 :175-293

[10] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY OF CARBOHYDRATES [J].

HICKS, KB .

ADVANCES IN CARBOHYDRATE CHEMISTRY AND BIOCHEMISTRY, 1988, 46 :17-72