A REVIEW OF METHODS FOR THE DETERMINATION OF HOLD-UP VOLUME IN MODERN LIQUID-CHROMATOGRAPHY

被引：79

作者：

SMITH, RJ ^{[1
]}

NIEASS, CS ^{[1
]}

WAINWRIGHT, MS ^{[1
]}

机构：

[1] COMMONWEALTH IND GASES LTD,ALEXANDRIA,NSW 2015,AUSTRALIA

来源：

JOURNAL OF LIQUID CHROMATOGRAPHY | 1986年 / 9卷 / 07期

关键词：

OPTIMIZATION; -; Applications; SEPARATION;

D O I：

10.1080/01483918608076694

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Arguably, the most important parameter in modern liquid chromatography is the hold-up (or dead) volume, V//M, the volume of mobile phase contained within the chromatographic system between the sample injector and the detector. Without this knowledge many dependent parameters such as capacity factor (k), selectivity (a), and resolution (R//S) cannot be computed. These data are of the utmost importance for the optimization of conditions for the separation of complex mixtures and the identification of solute bands.

引用

页码：1387 / 1430

页数：44

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