SYNTHESIS AND CHARACTERIZATION OF C-60(CCL4)(10)

被引:14
作者
GANGOPADHYAY, AK [1 ]
SCHILLING, JS [1 ]
DELEO, M [1 ]
BUHRO, WE [1 ]
ROBINSON, K [1 ]
KOWALEWSKI, T [1 ]
机构
[1] WASHINGTON UNIV,DEPT CHEM,ST LOUIS,MO 63130
关键词
FULLERENES; CHEMICAL SYNTHESIS; CRYSTAL GROWTH; CRYSTAL STRUCTURE AND SYMMETRY; THERMODYNAMIC PROPERTIES;
D O I
10.1016/0038-1098(95)00436-X
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
A new type of CCl4-solvated-C-60 compound has been synthesized in single crystal form which is stable at room temperature and below only when in contact with the C-60 saturated CCl4 solution. From differential scanning calorimetry (DSC) measurements we conclude that the crystal contains (10+/-2) CCl4 molecules per C-60 The crystal structure is face-centered-cubic (f.c.c.) with a lattice parameter of 27.39 Angstrom at room temperature.
引用
收藏
页码:597 / 600
页数:4
相关论文
共 12 条
[1]   FULLERENE C-60, 2CCL4 SOLVATE - A SOLID-STATE STUDY [J].
CEOLIN, R ;
AGAFONOV, V ;
ANDRE, D ;
DWORKIN, A ;
SZWARC, H ;
DUGUE, J ;
KEITA, B ;
NADJO, L ;
FABRE, C ;
RASSAT, A .
CHEMICAL PHYSICS LETTERS, 1993, 208 (3-4) :259-262
[2]   PSEUDOTENFOLD SYMMETRY IN PENTANE-SOLVATED C60 AND C70 [J].
FLEMING, RM ;
KORTAN, AR ;
HESSEN, B ;
SIEGRIST, T ;
THIEL, FA ;
MARSH, P ;
HADDON, RC ;
TYCKO, R ;
DABBAGH, G ;
KAPLAN, ML ;
MUJSCE, AM .
PHYSICAL REVIEW B, 1991, 44 (02) :888-891
[3]   STRUCTURE, DYNAMICS AND ORDERING TRANSITION OF SOLID C-60 [J].
HEINEY, PA .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1992, 53 (11) :1333-1352
[4]   STRUCTURE AND SUPERCONDUCTIVITY OF SINGLE CRYSTALLINE C60 [J].
KIKUCHI, K ;
SUZUKI, S ;
SAITO, K ;
SHIROMARU, H ;
IKEMOTO, I ;
ACHIBA, Y .
PHYSICA C, 1991, 185 :415-416
[5]   SOLID C-60 - A NEW FORM OF CARBON [J].
KRATSCHMER, W ;
LAMB, LD ;
FOSTIROPOULOS, K ;
HUFFMAN, DR .
NATURE, 1990, 347 (6291) :354-358
[6]  
LIDE DR, 1990, CRC HDB CHEM PHYSICS
[7]   SINGLE-CRYSTAL X-RAY STRUCTURE OF BENZENE-SOLVATED-C-60 [J].
MEIDINE, MF ;
HITCHCOCK, PB ;
KROTO, HW ;
TAYLOR, R ;
WALTON, DRM .
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1992, (20) :1534-1537
[8]   THERMODYNAMIC STUDY OF PHASE-TRANSITIONS IN CARBON-TETRACHLORIDE [J].
MORRISON, JA ;
RICHARDS, EL .
JOURNAL OF CHEMICAL THERMODYNAMICS, 1976, 8 (11) :1033-1038
[9]   STRUCTURE AND STABILITY OF CRYSTALLINE-C60-BULLET-N-PENTANE CLATHRATE [J].
PEKKER, S ;
FAIGEL, G ;
FODORCSORBA, K ;
GRANASY, L ;
JAKAB, E ;
TEGZE, M .
SOLID STATE COMMUNICATIONS, 1992, 83 (06) :423-426
[10]  
SCRIVENS WA, 1992, J AM CHEM SOC, V20, P7917