UV SPECTROPHOTOMETRIC DETERMINATION OF THEOBROMINE AND CAFFEINE IN COCOA BEANS

被引:24
作者
LI, S [1 ]
BERGER, J [1 ]
HARTLAND, S [1 ]
机构
[1] SWISS FED INST TECHNOL,DEPT CHEM ENGN & IND CHEM,CH-8092 ZURICH,SWITZERLAND
关键词
D O I
10.1016/S0003-2670(00)81263-5
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A rapid, simple and accurate method for individually determining theobromine and caffeine in cocoa beans is presented. Caffeine alone is completely extracted into chloroform from an aqueous solution at a pH between 12.5 and 12.7, and can be determined by UV spectrophotometry at 275.9 nm. For the theobromine remaining in the aqueous solution, a wavelength of 272.7 nm is used. The results were reproducible with a relative standard deviation of about 0.65%. © 1990.
引用
收藏
页码:409 / 412
页数:4
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