CHARACTERIZATION OF SPIN-ON-GLASS USING FOURIER-TRANSFORM INFRARED-SPECTROSCOPY

被引:27
作者
WOO, MP
CAIN, JL
LEE, CO
机构
[1] Motorola Incorporated, Advanced Products Research, Development Laboratories, Austin
[2] VLSI Technology Incorporated, San Antonio
关键词
D O I
10.1149/1.2086361
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
Spin-on-glass (SOG) has been characterized using process control techniques that provide in-line monitoring capability. Film composition changes have been observed for different anneal temperatures (300°-1000°C) and ambients (oxygen. and nitrogen). Fourier transform infrared (FTIR) spectroscopy and x-ray photoelectron spectroscopy (XPS) show a reduction in organic content in the film after annealing at temperatures above 500°C. Area integration under the silicon dioxide peak in the FTIR spectrum indicates compositional changes begin at a critical temperature identified as approximately 500°C. Both FTIR and XPS data show further densification of SOG takes place at higher temperature anneals (700°-1000°C). Refractive index and film stress measurement data correlate well with FTIR and XPS results. © 1990, The Electrochemical Society, Inc. All rights reserved.
引用
收藏
页码:196 / 200
页数:5
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