RAPID-DETERMINATION OF CALCIUM, MAGNESIUM, IRON AND ZINC IN FLOURS USING FLOW-INJECTION FLAME ATOMIC-ABSORPTION SPECTROMETRY FOR SLURRY ATOMIZATION

被引:21
作者
VINAS, P [1 ]
CAMPILLO, N [1 ]
GARCIA, IL [1 ]
CORDOBA, MH [1 ]
机构
[1] UNIV MURCIA,FAC CHEM,DEPT ANALYT CHEM,E-30071 MURCIA,SPAIN
关键词
D O I
10.1016/0308-8146(93)90125-Y
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A procedure is described for the rapid determination of calcium, magnesium, iron and zinc in flours obtained from several grains and legumes (wheat, whole meal, maize, barley, rice, rye, vetch, soy bean and field bean) using flame atomic absorption spectrometry. Suspensions up to 3% m/V from the ground samples are directly introduced into the spectrometer using a simple flow injection manifold. Calibration is performed using aqueous standard solutions of the determinands. The results obtained with this procedure agree with those obtained by conventional dry-ashing followed by dissolution in acids. Results for two standard reference materials are also given.
引用
收藏
页码:307 / 311
页数:5
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