ANALYSIS OF BUTYLLITHIUM AT CONCENTRATIONS USED IN INITIATION OF POLYMERIZATION

被引：10

作者：

URWIN, JR

REED, PJ

机构：

[1] Department of Physical and Inorganic Chemistry, University of Adelaide, Adelaide

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1968年 / 15卷 / 01期

关键词：

D O I：

10.1016/S0022-328X(00)86317-2

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

An NMR method devised for analysis of n-butyllithium solutions is acceptably accurate down to concentration of 0.1 M. An ultraviolet method, involving calibration with solutions analyzed by the NMR technique, is accurate to within ±5% down to concentrations of 10-3 M. © 1968.

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